I'm in the process of ripping the 3M 5200FC off the aluminum rim on my 850T3.

I ripped 40 humps off and each and internally every one looked like the above image. That fast cure product looks like it's almost boiling as it cures.
I did mount a tire on the rim and it maintained pressure overnight but the extreme bubble pattern in the test specimens did not inspire any confidence. So off it goes. Trust me, removal is no fun.
It's riding season. Time to put the bike back together with a tube for the season and ride it. I'll try this project again next January when I have all the time in the world to fuss over it. One group member mentioned building up the product in 3 layers. I think that might be the key for the release of gas during curing. I'm also going to switch from fast cure to standard cure. I have a feeling it probably outgasses less. I'll do a test first!